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Beilstein J. Org. Chem. 2011, 7, 1342–1346, doi:10.3762/bjoc.7.158
Graphical Abstract
Scheme 1: Chemical structure of compound 1 and mass spectral analysis.
Scheme 2: Retrosynthetic analysis of (R)-1.
Scheme 3: (a) BnOH, H2SO4; NaNO2, AcOH; CH2N2, 35% in 3 steps. (b) TBDPSCl, imidazole, 100%. (c) Pd/C, H2; BH3...
Scheme 4: (a) 5% NaOH, 100%. (b) PBr3, 82%. (c) PPh3, 98%.
Scheme 5: (a) PCC, 96%. (b) LDA, 15, 72%. (c) DCC, DMAP, phenylethylamine, 80%. (d) Pd/C, H2, 100%. (e) TBAF,...